An NPDES Permit is required for a discharge of wastewater to waters of the United States (surface waters). This permit is issued by the state by delegated authority of the Clean Water Act (CWA 1972). Since waters of the United States are also waters of the state, NPDES permits are actually combined NPDES/state waste discharge permits issued under dual (State and Federal) authorities. NPDES permits are typically issued for a maximum of five years. The most important amendment to the CWA was the NPDES permit program. Technology‐based effluent limits backed by plants discharging pollutants through a pipe or a conveyance (also see Section 4.9.3Table 4.6).

Table 4.4 Laboratory analytical methods.

ParametersMethods
General Chemistry
TurbidityEPA Revised 1983: 180.1
ConductivityEPA Revised 1983: 120.1
AlkalinityEPA Revised 1983: 310.1
HardnessEPA Revised 1983: 130.1
FluorideEPA Revised 1983: 340.3
Fluoride (soil)EPA Revised 1983: 340.3
Solids
TSEPA Revised 1983: 160.3
TNVSEPA Revised 1983: 160.3
TSSEPA Revised 1983: 160.2
TNVSSEPA Revised 1983: 160.2
% SolidsAPHA, 1989: 2540G
% Volatile solidsEPA Revised 1983: 160.4
Oxygen Demand Parameters
BOD5EPA Revised 1983: 405.1
CODEPA Revised 1983: 410.1
TOC (water)EPA Revised 1983: 415.1
TOC (soil/sediment)EPA Revised 1983: 405.1
Nutrients
NH3‐NEPA Revised 1983: 350.1
NO2 + NO3‐NEPA Revised 1983: 353.2
P – totalEPA Revised 1983: 365.3
Organics
VOC (water)EPA Revised 1986: 8260
VOC (soil/sediment)EPA Revised 1986: 8240
BNAs (water)EPA Revised 1986: 8270
BNAs (soil/sediment)EPA Revised 1986: 8270
Dioxin/Furans (water)EPA Revised 1986: 8290
Pest/PCB (water)EPA Revised 1986: 8080
Pest (soil/sediment)EPA Revised 1986: 8080
PAH (water)EPA Revised 1986: 8310
Metals
PP Metals (water)EPA Revised 1986: 200 ‐ 299
PP Metals (soil/sediment)EPA Revised 1986: 200 ‐ 299
Aluminum – ICPEPA Revised 1986: 220.7
Miscellaneous
Oil and grease (water)EPA Revised 1983: 413.1
Oil and grease (soil/sediment)EPA Revised 1983: 413.1
Cyanide (total)EPA Revised 1983: 335.2
Cyanide (wk & dis)APHA, 1989: 4500 ‐CNI
Cyanide (wk & dis soil/sed)APHA, 1989: 4500 ‐CNI
Fecal Coliform MFAPHA, 1989: 9222D
Bioassays
Rainbow Trout, Salmonid (acute 100%)Ecology, 1981
Daphnia magna (acute)EPA, 1985
Ceriodaphnia (chronic)EPA, 1989: 1002
Fathead Minnow (chronic)EPA, 1989: 1000
Hyallela (acute)Nebekar, 1984
Microtox (acute)Beckman, 1982
Field Analysis
pHAPHA, 1985: 423
TemperatureAPHA, 1985: 212
Chlorine ResidueAPHA, 1985: 408E
Method Bibliography
APHA –AWWA‐WPCF, 1989, Standard Methods for the Examination of Water and Wastewater, 17th Edition.
Beckman Instruments, Inc., 1982. Microtox System Operating Manual.
Ecology, 1981. Static Acute Fish Toxicity Test, WDOE 80‐12, revised July 1981.
EPA, Revised 1983, Methods for Chemical Analysis of Water and Wastes, EPA‐600/4‐79‐020 (Rev. March, 1983)
EPA, 1985, Methods for Measuring the Acute Toxicity of Effluents to Freshwater and Marine Organisms, EPA/600/4‐85/013.
EPA, 1986: SW846. Test Methods for Evaluating Solid Waste Physical/Chemical Methods, SW‐846, 3rd. Ed., November, 1986.
EPA, 1989. Short‐term Methods for Estimating the Chronic Toxicity of Effluents and Receiving Waters to Freshwater Organisms, second ed. EPA/600/4‐89/100.
Nebeker, et al. 1984. “Biological Methods for Determining Toxicity of Contaminated Freshwater Sediments to Invertebrates.” Environmental Toxicology and Chemistry, Vol. 3, 617–630.

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